4-[(4-Bromophenyl)diazenyl]-2-ethoxyaniline

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(E)-N-(2,4-Dimeth­oxy­benzyl­idene)-4-ethoxyaniline

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ویراستار سنتز و ساختار بلوری ترکیبات باز شیف N-(3,4-dimethoxybenzylidene)-4-methoxyaniline (1) و N-(3,4-dimethoxybenzylidene)-4-ethoxyaniline (2)

New Schiff-base compounds N-(3,4-dimethoxybenzylidene)-4-methoxyaniline (1) and N-(3,4-dimethoxybenzylidene)-4-ethoxyaniline (2) were synthesized and characterized by elemental analyses (CHN) and FT-IR spectroscopic techniques. Crystal structures of 1 and 2 were obtained by single-crystal X-ray diffraction. Compound 1 crystallizes in the monoclinic, space group P21 with two independent molecule...

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4-(4-Chloro­phen­yl)-4-hy­droxy­piperidinium 2-(2-phenyl­eth­yl)benzoate

In the title compound, C(11)H(15)ClNO(+)·C(15)H(13)O(2) (-), the piperidinium ring adopts a chair conformation. In the crystal, cations and anions are connected by inter-molecular O-H⋯O and N-H⋯O hydrogen bonds, forming two-dimensional networks parallel to the bc plane. Furthermore, the crystal structure is stabilized by weak C-H⋯π inter-actions.

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2-(4-Meth­oxy­phen­yl)-4-oxo-4-phenyl­butane­nitrile

The title mol-ecule, C(17)H(15)NO(2), is twisted, the dihedral angle between the terminal benzene rings being 63.30 (6)°. In the crystal, C-H⋯O and C-H⋯N inter-actions lead to supra-molecular layers in the ab plane. These are connected along the c axis via C-H⋯π inter-actions.

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2-(4-Chloro­phen­yl)-4-oxo-4-phenyl­butane­nitrile

The title mol-ecule, C16H12ClNO, has a V-shaped conformation and the dihedral angle between the planes of the phenyl and benzene rings of 64.6 (1)°. No directional intermolecular interactions could be identified in the crystal.

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2011

ISSN: 1600-5368

DOI: 10.1107/s160053681104877x